تفاعل #1631

معادلة التفاعل

cyclohexylphosphinic acid, n-butyl ester

paraformaldehyde

→

title compound

Cyclohexylhydroxymethylphosphinic acid, n-butyl ester

ظروف التفاعل

المعالجة

1. 1
   أخرىPurification by chromatography
2. 2
   غسيلeluting with dichloromethane containing 5% methanol
3. 3
   أخرىgave an oil

الإجراء التجريبي

The title compound was prepared from cyclohexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

المصدر