تفاعل #155395

معادلة التفاعل

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةwas heated
2. 2
   درجة الحرارةat reflux for 90 mins
3. 3
   تركيزThe reaction mixture was concentrated under reduced pressure
4. 4
   أخرىto give an oil
5. 5
   أخرىyield 5.77 parts of the following structure

الإجراء التجريبي

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

المصدر