تفاعل #1552054

معادلة التفاعل

methyl-4-bromobenzoate

hydrazine monohydrate

→

white solid

المردود 67.0%

4-bromobenzohydrazide

المردود 67.0%

المذيبات

ethanol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةthe mixture was heated
2. 2
   workup.STIRRINGstirred at 78° C. for 5 hours
3. 3
   أخرىA solid obtained
4. 4
   غسيلwashed with water
5. 5
   ترشيحcollected by suction filtration

الإجراء التجريبي

First, 3.0 g (13.9 mmol) of methyl-4-bromobenzoate was put in a 100-mL three-neck flask, 10 mL of ethanol was added therein, and the mixture was stirred. Thereafter, 4.0 mL of hydrazine monohydrate was added therein, and the mixture was heated and stirred at 78° C. for 5 hours. A solid obtained washed with water and collected by suction filtration; thus, 2.0 g of a white solid of objective 4-bromobenzohydrazide was obtained (yield: 67%).

المصدر