تفاعل #1552050

معادلة التفاعل

1,8-octanediamine

triethylamine

furoyl chloride

→

N,N′-(octane-1,8-diyl)bis(furan-2-carboxamide)

ظروف التفاعل

المعالجة

1. 1
   أخرىThe resulting compound was purified by column chromatography (98:2 DCM:EtOAc)
2. 2
   أخرىthe product obtained as a white solid (21.5 g/92%)

الإجراء التجريبي

The general procedure was carried out using 1,8-octanediamine (10.0 g, 69.3 mmol), triethylamine (14.2 g, 141 mmol), DMAP (0.17 g, 1.35 mmol) and furoyl chloride (19.0 g, 146 mmol). The resulting compound was purified by column chromatography (98:2 DCM:EtOAc), and the product obtained as a white solid (21.5 g/92%).

المصدر