تفاعل #1552043
ord-5457b3292eac4bc197a3beacfcc105ba
معادلة التفاعل
N-methoxy-acrylamide
chloroformic acid vinyl ester
→
title compound
N-Methoxy-N-propenoylcarbamic acid vinyl ester
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىPurification by column chromatography on silica gel (PE:EE=9:1)
الإجراء التجريبي
The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.