تفاعل #1552022
ord-6fac8adbf5474dab8f47671695980718
معادلة التفاعل
iodine monochloride
1-chloro-9-iodoperfluorononane
perfluorocyclopropane
1-chloro-11-iodoperfluoroundecane
→
1-chloro-3-iodoperfluoropropane
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىcan be obtained
الإجراء التجريبي
As for a compound in which n is 9 or 11 in formula (22), 1-chloro-9-iodoperfluorononane (22-4) or 1-chloro-11-iodoperfluoroundecane (22-5) can be obtained by allowing iodine monochloride to react with commercially available perfluorocyclopropane (53) at a high temperature to obtain 1-chloro-3-iodoperfluoropropane (54), and then allowing 1-chloro-3-iodoperfluoropropane (54) to react with tetrafluoroethylene (51) under high temperature and pressurized conditions.