تفاعل #1519114

معادلة التفاعل

3-aminocarbonylpropionate

hydroxylamine

→

N-hydroxy-3-aminocarbonylpropionamide

المذيبات

dioxane

ظروف التفاعل

المعالجة

1. 1
   أخرىpurified by preparative reverse-phase (C18) HPLC

الإجراء التجريبي

3-aminocarbonylpropionate A-6 (0.1 mmol) is treated with dioxane (1 mL) and hydroxylamine (50% in water, 2 mL) for 1-3 days, and then purified by preparative reverse-phase (C18) HPLC to afford the desired N-hydroxy-3-aminocarbonylpropionamide (A-7).

المصدر