تفاعل #1518

معادلة التفاعل

4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester

hydrogen

→

4-(6-decyloxy-2-naphthoyloxy)benzoic acid

المردود 97.5%

المذيبات

THF

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltered

الإجراء التجريبي

To 37.6 g (0.07 mol) of the 4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester obtained in the first stage was added 3.76 g of 5% palladium/carbon, and further added 188 g of THF. Then, hydrogen gas was blown into the mixture. The resultant mixture was stirred overnight and filtered to obtain 30.6 g of 4-(6-decyloxy-2-naphthoyloxy)benzoic acid.

المصدر