تفاعل #1381627
ord-ddecc81dca0e455d8001062829ecfc78
معادلة التفاعل
المتفاعلات
الكواشف
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىcrystallized three times from several volumes of acetone at 1° C.
الإجراء التجريبي
Erythritol and a five-fold molar excess of methyl oleate are heated at 180° C. under vacuum, with agitation, in the presence of sodium methoxide catalyst over two reaction periods of several hours each. The reaction product (predominately erytiritol tetraoleate) is refined in petroleum ether and crystallized three times from several volumes of acetone at 1° C.