تفاعل #1350565

معادلة التفاعل

N-butyl-N-cyclooctylpyrrolidinium iodide salt

hydroxide

→

N-butyl-N-cyclooctylpyrrolidinium hydroxide

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   workup.ADDITIONof Ion Exchange Resin OH (BIO RAD® AG1-X8) was added
2. 2
   ترشيحThe mixture was filtered
3. 3
   غسيلthe solids were rinsed with an additional 250 ml
4. 4
   ترشيحThe original mixture was filtered

الإجراء التجريبي

N-butyl-N-cyclooctylpyrrolidinium iodide salt (95 gms., 0.26 mole) was dissolved in 300 ml. water in a 1000 ml. plastic bottle. To the solution, 300 gms. of Ion Exchange Resin OH (BIO RAD® AG1-X8) was added and the mixture was stirred at room temperature overnight. The mixture was filtered and the solids were rinsed with an additional 250 ml. of water. The original mixture was filtered and the rinse were combined and a small amount was titrated with 0.1N HCl to indicate the presence of 0.24 mol hydroxide (0.24 mol N-butyl-N-cyclooctylpyrrolidinium hydroxide) in the solution.

المصدر