تفاعل #1340597

معادلة التفاعل

5-aminosalicylic acid

3-(4-nitrophenyl)propyl bromide

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2-hydroxy-5-[3-(4-nitrophenyl)-n-propylamino]-benzoic acid

المردود 50.4%

ظروف التفاعل

المعالجة

1. 1
   أخرىAccording to the similar procedure to Synthesis Example 1

الإجراء التجريبي

According to the similar procedure to Synthesis Example 1, by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 3-(4-nitrophenyl)propyl bromide (950 mg, 3.92 mmole), 520 mg (50% yield) of 2-hydroxy-5-[3-(4-nitrophenyl)-n-propylamino]-benzoic acid was obtained as a pale yellow solid. Melting point 229-231° C.

المصدر