تفاعل #1340563
ord-50762937bfe84de5b8de680d0acea52e
معادلة التفاعل
Triphenylene
AlCl3
CH3COCl
→
acetyltriphenylene
المردود 97.0%
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
Triphenylene (1 equivalent) is reacted at 0° C. with 2.1 equivalents of AlCl3 and 21.0 equivalents of CH3COCl in CH2Cl2. After stirring at room temp. for 3 hours, the reaction product (acetyltriphenylene) was obtained in 97% yield, and is used in step b).