تفاعل #1273146

معادلة التفاعل

octadecylmethacrylate

2-mercaptoethanol

→

Hexadecylmethacrylate Octadecylmethacrylate

المذيبات

toluene

toluene

ظروف التفاعل

المعالجة

1. 1
   workup.ADDITIONare slowly added to the reaction flask
2. 2
   درجة الحرارةwith continuous agitation, while the temperature is maintained

الإجراء التجريبي

A monomer feed containing 55 g of hexadecylmethacrylate, 55 g octadecylmethacrylate, 68 g toluene, and 0.58 g 2-mercaptoethanol, and an initiator feed containing 40 g toluene and 1.65 g 2,2′-azobis-2-methylpropionitrile are slowly added to the reaction flask, using the separator funnels, over a period of two hours, with continuous agitation, while the temperature is maintained at reflux (110° C.), under a flow of nitrogen.

المصدر