تفاعل #1265375

معادلة التفاعل

4-vinylbenzylchloride

morpholine

→

product

المردود 86.4%

N-(4-Vinylphenyl)methylmorpholine

المردود 86.4%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   تركيزThe mixture was then concentrated in vacuo
2. 2
   أخرىthe resulting residue was partitioned between 1M hydrochloric acid and water [sic]
3. 3
   غسيلThe acidic phase was washed with ether
4. 4
   استخلاصThis aqueous phase was extracted with ether
5. 5
   أخرىThis organic phase was dried
6. 6
   تركيزconcentrated in vacuo

الإجراء التجريبي

20 ml (0.14 mol) of 4-vinylbenzylchloride and 25 ml (0.28 mol) of morpholine were refluxed in 150 ml of methanol for 3 h. The mixture was then concentrated in vacuo, and the resulting residue was partitioned between 1M hydrochloric acid and water [sic]. The acidic phase was washed with ether and then made alkaline with 2M sodium hydroxide solution. This aqueous phase was extracted with ether. This organic phase was dried and concentrated in vacuo, resulting in 24.6 g of the product.

المصدر