تفاعل #1255206

معادلة التفاعل

Diphenyliodonium chloride

trimethyl phosphate

→

target compound

المردود 81.6%

diphenyliodonium dimethylphosphonate

المردود 81.6%

ظروف التفاعل

المعالجة

1. 1
   workup.DISSOLUTIONAfter the reactants were dissolved
2. 2
   درجة الحرارةthe mixture was cooled
3. 3
   أخرىto thereby yield solid matter
4. 4
   غسيلThe solid matter was washed with ether

الإجراء التجريبي

Diphenyliodonium chloride (315 mg; 1 mmol) and trimethyl phosphate (1 g) were stirred at 170° C. for 10 minutes. After the reactants were dissolved, the mixture was cooled, to thereby yield solid matter. The solid matter was washed with ether, to thereby yield 250 mg of the target compound as white crystals (yield: 81.6%). The anion content of the resultant compound was determined by ion chromatography. The chloride anion content was determined to be not greater than 10 ppm.

المصدر