تفاعل #11956

معادلة التفاعل

compound

Nα-Fmoc-Nδ-Boc-L-ornithine

diethylamine

→

title compound

Nδ-Boc-L-ornithine

المذيبات

DMF

ظروف التفاعل

المعالجة

1. 1
   أخرىAfter the reaction
2. 2
   أخرىthe solvent was removed by distillation under reduced pressure
3. 3
   أخرىthe residue was dried under vacuum

الإجراء التجريبي

The compound obtained in Example 23-1 (250.8 mg) was dissolved in DMF (5 ml). After the addition of diethylamine. (0.5 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (269.1 mg).

المصدر