تفاعل #1192972
ord-48642f58e3b84aca8818938e77021646
معادلة التفاعل
hexafluorophosphoric acid
diphenyliodonium chloride
fluoroboric acid
→
diphenyliodonium hexafluorophosphate
المردود 74.0%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The procedure of Example 1 was repeated for preparing an aromatic halonium salt using diphenyliodonium chloride. In this preparation, fluoroboric acid was replaced by 25 ml (60%) hexafluorophosphoric acid. There was obtained a 74% yield of diphenyliodonium hexafluorophosphate having a m.p. of 139°-141° C.