تفاعل #1106669

ord-f5ff3aa120644be0be915121f0436399

معادلة التفاعل

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin
COCCNc1cccc2c1C(=O)c1cccc(NCCN(C)C)c1C2=O
2-(dimethylamino) ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis product was used in the next step without any purification

الإجراء التجريبي

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08715944B2uspto-grants-2014_05