تفاعل #1106665

معادلة التفاعل

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةwas refluxed for 18 h
2. 2
   أخرىto precipitate the title compound which
3. 3
   أخرىwas recrystallised from methanol

الإجراء التجريبي

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

المصدر