تفاعل #1095849

معادلة التفاعل

Urocanic acid

urocanic acid

→

3-(1H-Imidazol-4-yl)propionic acid

المذيبات

MeOH

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltered
2. 2
   تركيزthe filtrate was concentrated under a reduced pressure
3. 3
   أخرىto give the objective product

الإجراء التجريبي

Urocanic acid (3-(1H-imidazol-4-yl)-acrylic acid) (138 mg, 1 mmol) was placed in a round-bottom flask and dist MeOH was added thereto until urocanic acid was completely dissolved. To this solution, 10% Pd/C (30 mg) was added, replaced with H2 and stirred. After five hours, the loss of raw materials was confirmed, filtered, and the filtrate was concentrated under a reduced pressure to give the objective product.

المصدر