تفاعل #1094808

معادلة التفاعل

4-vinylcyclohexene-1,2-epoxide

water

sulfuric acid

→

1,2-dihydroxy-4-vinylcyclohexane

المذيبات

acetone

ظروف التفاعل

المعالجة

1. 1
   أخرىInto a two-neck flask (100 ml) were fed
2. 2
   أخرىAfter complete reaction
3. 3
   استخلاصan object compound was extracted with each 60 ml of diethylether four times
4. 4
   غسيلwas washed with saturated salt solution
5. 5
   تجفيفwas dried with sodium sulfate
6. 6
   أخرىThe solvent was evaporated

الإجراء التجريبي

Into a two-neck flask (100 ml) were fed 15.9 g (128 mmol) of 4-vinylcyclohexene-1,2-epoxide, 40 ml of water, 20 ml of acetone, and 40 μl of sulfuric acid, and the reaction mixture was refluxed at 75° C. for 4 hours. After complete reaction, an object compound was extracted with each 60 ml of diethylether four times, and was washed with saturated salt solution, and then was dried with sodium sulfate. The solvent was evaporated to obtain 1,2-dihydroxy-4-vinylcyclohexane.

المصدر