تفاعل #1073160

ord-9294e126bd8b47b9b7be998f2dfcd389

معادلة التفاعل

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCCCCCCCCCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Dodecyl-N-(2-amino-2-deoxy-glucopyranosyl)-amine hydrochloride

المتفاعلات

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.ADDITIONwere added
  2. 2
    أخرىthe product precipitated
  3. 3
    استخلاصThe solid was extracted three times
  4. 4
    workup.STIRRINGby stirring with ether
  5. 5
    ترشيحfiltered off with suction
  6. 6
    أخرىdried under a high vacuum

الإجراء التجريبي

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04710491uspto-grants-1987_12