تفاعل #10580

معادلة التفاعل

disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate

calcium chloride dihydrate

→

Calcium bicyclo[2.2.1]heptane-2,3-dicarboxylate

المذيبات

water

water

ظروف التفاعل

المعالجة

1. 1
   ترشيحThe resulting white precipitate was filtered
2. 2
   أخرىThe white powdery product was dried
3. 3
   أخرىmilled (m.p. >300° C.)

الإجراء التجريبي

To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).

المصدر