تفاعل #10544
ord-a37b355baf0d4ccb87189a29d7e7e818
المتفاعلات
الكواشف
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1workup.STIRRINGAfter stirring for 16 hours the reaction mixture
- 2ترشيحwas filtered through Arbocel (trade mark)
- 3أخرىthe solvent removed under reduced pressure
الإجراء التجريبي
Peariman's catalyst (20% w/w palladium hydroxide-on-carbon) (1.5 g) was added to a solution of cyclopentylamine (15 ml, 0.21 mol) in acetone (200 ml). The reaction mixture was stirred under an atmosphere of hydrogen gas at 414 kPa (60 psi). After stirring for 16 hours the reaction mixture was filtered through Arbocel (trade mark) and the solvent removed under reduced pressure to give the title compound (15 ml) as a thin oil.