تفاعل #10544

ord-a37b355baf0d4ccb87189a29d7e7e818

المتفاعلات

الكواشف

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.STIRRINGAfter stirring for 16 hours the reaction mixture
  2. 2
    ترشيحwas filtered through Arbocel (trade mark)
  3. 3
    أخرىthe solvent removed under reduced pressure

الإجراء التجريبي

Peariman's catalyst (20% w/w palladium hydroxide-on-carbon) (1.5 g) was added to a solution of cyclopentylamine (15 ml, 0.21 mol) in acetone (200 ml). The reaction mixture was stirred under an atmosphere of hydrogen gas at 414 kPa (60 psi). After stirring for 16 hours the reaction mixture was filtered through Arbocel (trade mark) and the solvent removed under reduced pressure to give the title compound (15 ml) as a thin oil.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07094769B2uspto-grants-2006_08